1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

Base Information

Chemical Name:1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane
CAS No.:76820-12-7
Molecular Formula:C₃₄H₃₆O₇
Molecular Weight:556.656
Hs Code.:

Synonyms:1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

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Technology Process of 1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

There total 2 articles about 1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 105-39-5
chloroacetic acid ethyl ester

: 76799-30-9
1-<2,6-bis(benzyloxy)-4-hydroxyphenyl>-3-<3-(benzyloxy)-4-methoxyphenyl>propane

: 76820-12-7
1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 22h;
DOI:10.1021/jm00136a011

Reference yield:

: 63240-52-8
2,3',6-tris(benzyloxy)-4-hydroxy-4'-methoxydihydrochalcone

: 76820-12-7
1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LiAlH₄ / 1,2-dimethoxy-ethane / 2.5 h / Heating

2: 100 percent / K₂CO₃ / dimethylformamide / 22 h / 40 °C

With lithium aluminium tetrahydride; potassium carbonate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011

Reference yield: 100.0%

: 76820-12-7
1-<2,6-bis(benzyloxy)-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

: 1-<2,6-dihydroxy-4-(carbethoxymethoxy)phenyl>-3-(3-hydroxy-4-methoxyphenyl)propane

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 22h; under 3040 Torr; Ambient temperature;
DOI:10.1021/jm00136a011