Bicyclo[1.1.1]pentane-1-carboxylic acid, 3-fluoro-, methyl ester (9CI)

Base Information

• Chemical Name: Bicyclo[1.1.1]pentane-1-carboxylic acid, 3-fluoro-, methyl ester (9CI)
• CAS No.: 262851-99-0
• Molecular Formula: C₇H₉FO₂
• Molecular Weight: 144.146
• Mol file: 262851-99-0.mol

Synonyms:3-Fluorobicyclo[1.1.1]pentane-1-carboxylicacid methyl ester

Chemical Property of Bicyclo[1.1.1]pentane-1-carboxylic acid, 3-fluoro-, methyl ester (9CI)

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

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Technology Process of Bicyclo[1.1.1]pentane-1-carboxylic acid, 3-fluoro-, methyl ester (9CI)

There total 2 articles about Bicyclo[1.1.1]pentane-1-carboxylic acid, 3-fluoro-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3‐(methoxycarbonyl)bicyclo[1.1.1]pentane‐1‐carboxylic acid (83249-10-9) → 3-fluoro-bicyclo[1.1.1]pentane-1-carboxylic acid methyl ester (262851-99-0)

Guidance literature:

With silver nitrate; Selectfluor; In water; at 65 ℃; for 16h; Inert atmosphere;

DOI:10.1039/c5ob02066b

Reference yield:

3‐(methoxycarbonyl)bicyclo[1.1.1]pentane‐1‐carboxylic acid (83249-10-9) → dimethyl <2>staffane-3,3'-dicarboxylate (131515-47-4) + 3-fluoro-bicyclo[1.1.1]pentane-1-carboxylic acid methyl ester (262851-99-0) + C7H9(2)HO2

Guidance literature:

With xenon difluoride; In dichloromethane-d2; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/jo982124o

Reference yield: 32.0%

3-fluoro-bicyclo[1.1.1]pentane-1-carboxylic acid methyl ester (262851-99-0) → 3-fluorobicyclo<1.1.1>pentane-1-carboxylic acid (146038-53-1)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; at 50 ℃; for 16h; Inert atmosphere;

DOI:10.1039/c5ob02066b

upstream raw materials:

3‐(methoxycarbonyl)bicyclo[1.1.1]pentane‐1‐carboxylic acid

Downstream raw materials:

3-fluorobicyclo<1.1.1>pentane-1-carboxylic acid

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