N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Base Information

Chemical Name:N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide
CAS No.:171179-60-5
Molecular Formula:C₁₄H₁₇N₅O₅
Molecular Weight:335.319
Hs Code.:

Synonyms:N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Suppliers and Price of N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

There total 6 articles about N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 27715-62-4
5-methyl-2,4-dinitrobenzamide

: 171179-60-5
N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Guidance literature:: In N,N-dimethyl-formamide; at 25 ℃; for 1h;
DOI:10.1021/jo951790b

Reference yield:

: 3113-71-1
3-methyl-4-nitrobenzoic acid

: 171179-60-5
N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / conc. H₂SO₄ / 24 h / Heating

2: 70 percent / conc. H₂SO₄, fuming HNO₃ / 138 h / -20 °C

3: 90 percent / NH₃ / methanol / 12 h / 80 °C

4: 84 percent / dimethylformamide / 1 h / 25 °C

With sulfuric acid; ammonia; nitric acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo951790b

Reference yield:

: 3113-72-2
5-methyl-2-nitrobenzoic acid

: 171179-60-5
N-<(dimethylamino)methylene>-(E)-5-<2-(dimethylamino)ethenyl>-2,4-dinitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / conc. H₂SO₄ / 48 h / Heating

2: 30 percent / CF₃SO₃H, fuming HNO₃ / CH₂Cl₂ / 20 h / 25 °C

3: 90 percent / NH₃ / methanol / 12 h / 80 °C

4: 84 percent / dimethylformamide / 1 h / 25 °C

With trifluorormethanesulfonic acid; sulfuric acid; ammonia; nitric acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo951790b