C₁₅H₂₂FN₃O₂S

Base Information

Chemical Name:C₁₅H₂₂FN₃O₂S
CAS No.:1248504-06-4
Molecular Formula:C₁₅H₂₂FN₃O₂S
Molecular Weight:327.423
Hs Code.:

C<sub>15</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>2</sub>S

Synonyms:C₁₅H₂₂FN₃O₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₂FN₃O₂S

Chemical Property:

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Technology Process of C₁₅H₂₂FN₃O₂S

There total 9 articles about C₁₅H₂₂FN₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₀FN₃O₂S

: 74-88-4
methyl iodide

: 1248504-06-4
C₁₅H₂₂FN₃O₂S

Guidance literature:: In acetonitrile; at 60 ℃; for 3h;

Reference yield:

: 79110-05-7
1-(2-fluoro-5-nitrophenyl)ethanone

: 1248504-06-4
C₁₅H₂₂FN₃O₂S

Guidance literature:: Multi-step reaction with 9 steps

1: water; ammonium chloride; iron / ethanol; tetrahydrofuran / 2 h / 20 - 70 °C

2: dmap; triethylamine / dichloromethane / 20 °C

3: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

4: triethylamine / dichloromethane / 1.5 h / 20 °C

5: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

6: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

7: tetrahydrofuran / 0.5 h / 20 °C

8: sodium hydroxide; water / methanol / 0.42 h / 50 °C

9: acetonitrile / 3 h / 60 °C

With dmap; sodium tetrahydroborate; sodium azide; water; iron; ammonium chloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 386216-31-5
(3-acetyl-4-fluorophenyl)carbamic acid tert-butyl ester

: 1248504-06-4
C₁₅H₂₂FN₃O₂S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

2: triethylamine / dichloromethane / 1.5 h / 20 °C

3: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

4: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

5: tetrahydrofuran / 0.5 h / 20 °C

6: sodium hydroxide; water / methanol / 0.42 h / 50 °C

7: acetonitrile / 3 h / 60 °C

With sodium tetrahydroborate; sodium azide; water; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;