(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

Base Information

Chemical Name:(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester
CAS No.:192371-86-1
Molecular Formula:C₂₄H₂₄NO₃PS
Molecular Weight:437.499
Hs Code.:

Synonyms:(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

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Chemical Property of (S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

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Technology Process of (S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

There total 1 articles about (S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 109602-95-1
3-(diphenylphosphorothioyl)propionic acid

: 6591-61-3,24461-61-8,26682-99-5,37760-98-8
(S)-Phenylglycine methyl ester

: 192371-86-1
(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; acetonitrile; Ambient temperature;
DOI:10.1039/a607200c

Reference yield:

: 192371-86-1
(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

: 216863-09-1
3-(Diphenyl-phosphinothioyl)-N-((S)-2-hydroxy-1-phenyl-ethyl)-propionamide

Guidance literature:: With lithium borohydride; In tetrahydrofuran;
DOI:10.1039/a607200c

Reference yield:

: 192371-86-1
(S)-[3-(Diphenyl-phosphinothioyl)-propionylamino]-phenyl-acetic acid methyl ester

: (S)-2-(2-Diphenylphosphanyl-ethyl)-4-phenyl-4,5-dihydro-oxazole

Guidance literature:: Multi-step reaction with 3 steps

1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2: CH₃O₂CNSO₂N(C₂H₅)3 / tetrahydrofuran / 1 h / Heating; other reagent: triethylamine/mesyl chloride

3: Raney nickel / methanol / 8 h / Ambient temperature

With lithium borohydride; Burgess Reagent; nickel; In tetrahydrofuran; methanol;
DOI:10.1021/jo981420y