3-(Diphenylphosphorothioyl)propanoic acid

Base Information

Chemical Name:3-(Diphenylphosphorothioyl)propanoic acid
CAS No.:109602-95-1
Molecular Formula:C15H15O2PS
Molecular Weight:290.323
Hs Code.:
DSSTox Substance ID:DTXSID90572403
Wikidata:Q82460751

Synonyms:109602-95-1;3-(Diphenylphosphorothioyl)propanoic acid;DTXSID90572403

Suppliers and Price of 3-(Diphenylphosphorothioyl)propanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-(Diphenylphosphorothioyl)propanoic acid

Chemical Property:

Melting Point:128 °C
Boiling Point:465.3±47.0 °C(Predicted)
PSA：79.20000
Density:1.27±0.1 g/cm3(Predicted)
LogP:3.24220
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:290.05303789
Heavy Atom Count:19
Complexity:322

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=S)(CCC(=O)O)C2=CC=CC=C2

Technology Process of 3-(Diphenylphosphorothioyl)propanoic acid

There total 3 articles about 3-(Diphenylphosphorothioyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 2848-01-3
3-(diphenylphosphino)propionic acid

: 109602-95-1
3-(diphenylphosphorothioyl)propionic acid

Guidance literature:: With sulfur; In toluene; for 2h; Inert atmosphere; Reflux;
DOI:10.1039/c5dt01796c

Reference yield:

: 829-85-6
diphenylphosphane

: 109602-95-1
3-(diphenylphosphorothioyl)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Me₄NOH / acetonitrile / 12 h / Ambient temperature

2: Na₂S₂O₃ / methanol / 12 h / 46 °C

With tetramethyl ammoniumhydroxide; sodium thiosulfate; In methanol; acetonitrile;