(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

Base Information

Chemical Name:(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone
CAS No.:249762-50-3
Molecular Formula:C₃₀H₂₂N₂O₆S₂
Molecular Weight:570.646
Hs Code.:

Synonyms:(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

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Chemical Property of (6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

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Technology Process of (6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

There total 5 articles about (6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 249762-35-4
(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanol

: 249762-50-3
(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

Guidance literature:: With dipyridinium dichromate; pyridinium trifluroacetate; In dichloromethane; at 20 ℃;
DOI:10.1021/jm010988n

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 1-benzenesulfonyl-6-methoxy-1H-indole-2-carbonyl chloride

: 249762-50-3
(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

Guidance literature:: 1-benzenesulfonylindole; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

1-benzenesulfonyl-6-methoxy-1H-indole-2-carbonyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jm010988n

Reference yield:

: 56995-13-2
6-methoxy-1-(phenylsulfonyl)-1H-indole

: 249762-50-3
(6-methoxy-1-phenylsulfonyl-1H-2-indolyl)(1-phenylsulfonyl-1H-2-indolyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi; iPr₂NH / tetrahydrofuran / 1 h / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

1.3: 6N HCl / CH₂Cl₂ / 1 h / Heating

2.1: thionyl chloride / 1 h / Heating

3.1: n-Buli; iPr₂NH / tetrahydrofuran / 0.5 h / 0 °C

3.2: tetrahydrofuran / -78 - 20 °C

With n-butyllithium; thionyl chloride; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/jm010988n