[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O

Base Information

• Chemical Name: [Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O
• CAS No.: 87183-71-9
• Molecular Formula: C₁₀H₂₂CoN₅O₇P*ClO₄*H₂O
• Molecular Weight: 531.747

Synonyms:[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O

Chemical Property of [Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O

Chemical Property:

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Technology Process of [Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O

There total 1 articles about [Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Co(NH2CH2CH2NH2)2(O3POC6H5)]2(2+)*2CF3SO3(1-)=[Co(NH2CH2CH2NH2)2(O3POC6H5)]2(SO3CF3)2 + sodium perchlorate → [Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)](1+)*ClO4(1-)*H2O=[Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)]ClO4*H2O (87183-71-9)

Guidance literature:

With water; nitric acid; In further solvent(s); Co complex added in portion to stirred ice-cold triflic acid, after allof solid dissolved rapidly added concd. HNO3, stirred for 10 min; soln. added to Et2O, stirred for 20 min, Et2O decanted and Et2O added, gum dissolved in H2O, Et2O washes extd. with H2O, to aq. soln. added NaOH (pH 2.5), chromd. (Sephadex C-25 resin, NaClO4) added aq. NH3, cooled,ppt. washed,dried in vac.; elem. anal.;

DOI:10.1021/ja00363a021

Reference yield: 90.0%

ammonium p-toluenesulfonate (4124-42-9) + [Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)](1+)*ClO4(1-)*H2O=[Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)]ClO4*H2O (87183-71-9) + 18O-labeled water (14797-71-8) → [Co(NH2CH2CH2NH2)2(((18)O)H2)(O3POC6H4NO2)](1+)*C7H7SO3(1-)=[Co(NH2CH2CH2NH2)2(((18)O)H2)(O3POC6H4NO2)]SO3C6H4CH3 (87183-73-1)

Guidance literature:

With trifluorormethanesulfonic acid; ammonia; In further solvent(s); to suspn. of Co complex in (((18)O)H2) added CF3SO3H (pH 1.5), warmed to 50 .deghree.C, stirred until all of solid dissolved, allowed to stand at room temp. for 4 d, filtered, pH filtrate adjusted to 4-5 (concd. aq.NH3), added NH4SO3C6H4CH3; pptd. by cooling at 0 ° C for 2 h, ppt. washed ice-cold H2O, allowed to dry in air for 20 min, anhyd. product obtained by desication in vac. over P2O5 over 18 h; elem. anal.;

DOI:10.1021/ja00363a021

Reference yield: 87.0%

[Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)](1+)*ClO4(1-)*H2O=[Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)]ClO4*H2O (87183-71-9) → [Co(ethylenediamine)2(H2O)2](3+) (18485-07-9,18485-08-0,19314-32-0,45837-92-1,21247-59-6,21242-06-8) + trans-aqua(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) ion (87183-70-8,93060-70-9) + Co(en)2(O2PO2)

Guidance literature:

With sodium perchlorate; 2,2'-iminobis[ethanol]; In water; byproducts: 4-nitrophenol, 4-nitrophenyl phosphate; to suspn. of Co complex in H2O added diethanolamine buffer ( amine concn. = 0.4 M, μ = 2 M, NaClO4) at 25 .gedree.C with stirring, stirred; added HClO4 until pH was 4,diluted with H2O and sorbed on Sephadex C-25resin (washed with ice-cold H2O at pH 3.5(acetate buffer)),washed with cold H2O,then NaClO4 (Co(en)2(OH2)O4PC6H4NO2(1+)), NH3 (Co(en)2PO4), NaClO4 at pH 9.5(NH3) (Co(en)2(OH2)2(3+)); Kinetics;

DOI:10.1021/ja00363a021

Downstream raw materials:

[Co(ethylenediamine)2(H₂O)2]⁽³⁺⁾

trans-aqua(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) ion

[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁷⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*SO₃C₆H₄CH₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁷⁾O)H₂)(O₃POC₆H₄NO₂)](SO₃C₆H₄CH₃)

[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃

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