N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

Base Information

Chemical Name:N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide
CAS No.:1421837-20-8
Molecular Formula:C₂₈H₂₇ClN₂O₃
Molecular Weight:474.987
Hs Code.:

Synonyms:N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

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Chemical Property of N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

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Technology Process of N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

There total 3 articles about N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.68%

: 118762-04-2
1-(4-chlorophenyl)-N-methyl-1-phenylmethanamine

: 744242-85-1
2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)acetic acid

: 1421837-20-8
N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

Guidance literature:: 2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)acetic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 2h;

1-(4-chlorophenyl)-N-methyl-1-phenylmethanamine; With benzotriazol-1-ol; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield: 50.68%

: 1421837-20-8
N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 28022-43-7
p-chlorobenzhydrylamine

: 1421837-20-8
N-((4-chlorophenyl)(phenyl)methyl)-2-(4-((3,5-dimethylisoxazol-4-yl)methoxy)phenyl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 2 h / 20 °C

2.2: 24 h / 20 °C

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;