S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate

Base Information

• Chemical Name: S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate
• CAS No.: 84774-90-3
• Molecular Formula: C₂₉H₂₇N₂O₆PS₄
• Molecular Weight: 658.781

Synonyms:S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate

Chemical Property of S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate

There total 4 articles about S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

cyclohexylammonium S,S-diphenyl phosphorodithioate (67941-87-1) + 5'-O-(1,3-benzodithiol-2-yl)thymidine (84752-63-6) → S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate (84774-90-3)

Guidance literature:

With 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; In pyridine; for 5h;

DOI:10.1021/ja00345a062

Reference yield:

2-(3-methylbutoxy)-1,3-benzodithiole (55315-56-5) → S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate (84774-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 53 percent / TsOH*H₂O, molecular sieves / dioxane / 1 h

2: 96 percent / BuNH₂ / methanol / 3 h / Ambient temperature

3: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

With molecular sieve; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; toluene-4-sulfonic acid; N-butylamine; In 1,4-dioxane; pyridine; methanol;

DOI:10.1021/ja00345a062

Reference yield:

3'-O-acetylthymidine (21090-30-2) → S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate (84774-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 53 percent / TsOH*H₂O, molecular sieves / dioxane / 1 h

2: 96 percent / BuNH₂ / methanol / 3 h / Ambient temperature

3: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

With molecular sieve; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; toluene-4-sulfonic acid; N-butylamine; In 1,4-dioxane; pyridine; methanol;

DOI:10.1021/ja00345a062

upstream raw materials:

cyclohexylammonium S,S-diphenyl phosphorodithioate

5'-O-(1,3-benzodithiol-2-yl)thymidine

2-(3-methylbutoxy)-1,3-benzodithiole

3'-O-acetylthymidine

Downstream raw materials:

C₄₅H₄₄N₄O₁₂P₂S₅

C₃₉H₃₉N₄O₁₃P₂S₄^(1-)

C₃₈H₄₀N₄O₁₂P₂S₃

S,S-diphenyl thymidine 3'-phosphorodithioate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 84774-90-3 S,S-diphenyl 5'-O-(1,3-benzodithiol-2-yl)thymidine 3'-phosphorodithioate

Send

Send

Metric Ton KG G Pound L ML

Send

Send