N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

Base Information

Chemical Name:N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride
CAS No.:1120334-10-2
Molecular Formula:C₁₄H₁₄N₄O₂*ClH
Molecular Weight:306.752
Hs Code.:

Synonyms:N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

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Chemical Property of N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

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Technology Process of N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

There total 3 articles about N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1122-62-9
2-acetylpyridine

: 100032-76-6
(2-nitro-4-methylphenyl)hydrazine hydrochloride

: 1120334-10-2
N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

Guidance literature:: With sodium acetate; In methanol; at 20 ℃; for 8h;

Reference yield: 82.0%

: 1122-62-9
2-acetylpyridine

: (2-nitro-4-methyl-phenyl)-hydrazine hydrochloride

: 1120334-10-2
N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

Guidance literature:: With sodium acetate; In methanol; at 20 ℃; for 8h;

Reference yield:

: 89-62-3
4-methyl-2-nitroaniline

: 1120334-10-2
N-[(4-methyl-2-nitrophenyl)]-N′-[1-(pyridin-2-yl)ethylidene]hydrazine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: sodium acetate / methanol / 8 h / 20 °C

With hydrogenchloride; sodium acetate; sodium nitrite; In methanol; water;