1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

Base Information

Chemical Name:1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene
CAS No.:959687-85-5
Molecular Formula:C₁₀H₁₀BrF₃O₂
Molecular Weight:299.087
Hs Code.:
Mol file:959687-85-5.mol

Synonyms:1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

Suppliers and Price of 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Labseeker
1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene 95
10g
$ 2383.00

American Custom Chemicals Corporation
1-BROMO-2-(DIMETHOXYMETHYL)-4-(TRIFLUOROMETHYL)BENZENE 95.00%
5MG
$ 505.93

Total 0 raw suppliers

Chemical Property of 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

Chemical Property:

Purity/Quality:: 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

There total 1 articles about 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 102684-91-3
2-bromo-5-(trifluoromethyl)benzaldehyde

: 149-73-5
trimethyl orthoformate

: 959687-85-5
1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

Guidance literature:: With sulfuric acid; In methanol; at 72 ℃; for 1h;
DOI:10.1016/j.bioorg.2021.105560

Reference yield: 94.0%

: 959687-85-5
1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

: 106-95-6
allyl bromide

: C₁₁H₉F₃O

Guidance literature:: 2-bromo-5-trifluoromethylbenzaldehyde dimethyl acetal; With magnesium; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at 0 - 80 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; for 72h; Inert atmosphere;
DOI:10.1039/c6cc01915c

Reference yield: 20.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 959687-85-5
1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene

: 7732-18-5
water

: 4-(trifluoromethyl)-2-formylphenylboronic acid

Guidance literature:: 1-bromo-2-(dimethoxymethyl)-4-(trifluoromethyl)benzene; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -70 - -65 ℃; for 1h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; diethyl ether; hexane; at -65 ℃; for 1h;

water; With hydrogenchloride; In tetrahydrofuran; diethyl ether; hexane; at 0 ℃; for 0.5h;
DOI:10.1016/j.bioorg.2021.105560