6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

Base Information

Chemical Name:6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)
CAS No.:1402143-03-6
Molecular Formula:C₂₃H₂₂N₂O₄
Molecular Weight:390.439
Hs Code.:

Synonyms:6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

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Chemical Property of 6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

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Technology Process of 6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

There total 1 articles about 6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 496-72-0
4-methyl-1,2-diaminobenzene

: 1402143-03-6
6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

Guidance literature:: In ethanol; for 4.5h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.inorgchem.0c01146

Reference yield: 87.5%

: 1402143-03-6
6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

: C₂₃H₂₀N₄O₆

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; Cooling;
DOI:10.1007/s12039-014-0728-3

Reference yield: 30.0%

: 1402143-03-6
6,6'-(4-methyl-1,2-phenylene)bis(azan-1-yl-1-ylidene)bis(2-methoxyphenol)

: neodymium(III) acetate hexahydrate

: 3C₂₃H₂₀N₂O₄^(2-)*3Nd⁽³⁺⁾*3C₂H₃O₂^(1-)

Guidance literature:: With triethylamine; In methanol; ethanol; for 0.5h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.inorgchem.0c01146