N-(4-methoxyphenyl)-2-propanamide

Base Information

Chemical Name:N-(4-methoxyphenyl)-2-propanamide
CAS No.:220903-58-2
Molecular Formula:C₁₃H₁₅F₃N₂O₃
Molecular Weight:304.269
Hs Code.:

N-(4-methoxyphenyl)-2-<N-(trifluoroacetyl)methylamino>propanamide

Synonyms:N-(4-methoxyphenyl)-2-propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-methoxyphenyl)-2-propanamide

Chemical Property:

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Technology Process of N-(4-methoxyphenyl)-2-propanamide

There total 3 articles about N-(4-methoxyphenyl)-2-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220903-53-7
2-amino-N-(4-methoxyphenyl)propanamide

: 220903-58-2
N-(4-methoxyphenyl)-2-propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / CH₂Cl₂

2: 1.) NaH / 1.) DMF, 20 deg C, 2 h, 2.) DMF, 20 deg C, 8h

With pyridine; sodium hydride; In dichloromethane;
DOI:10.1021/jm960783s

Reference yield:

: 220903-51-5
<(tert-butyloxycarbonyl)amino>-N-(4-methoxyphenyl)propanamide

: 220903-58-2
N-(4-methoxyphenyl)-2-propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / CF₃COOH / 1 h / 20 °C

2: 78 percent / pyridine / CH₂Cl₂

3: 1.) NaH / 1.) DMF, 20 deg C, 2 h, 2.) DMF, 20 deg C, 8h

With pyridine; sodium hydride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm960783s

Reference yield:

: 220903-57-1
N-(4-methoxyphenyl)-2-(trifluoroacetylamino)propanamide

: 74-88-4
methyl iodide

: 220903-58-2
N-(4-methoxyphenyl)-2-propanamide

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) DMF, 20 deg C, 2 h, 2.) DMF, 20 deg C, 8h;
DOI:10.1021/jm960783s