Technology Process of 6,7-Quinolinediamine
There total 6 articles about 6,7-Quinolinediamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
palladium on activated charcoal;
In
ethanol;
for 2.5h;
Heating;
DOI:10.3987/COM-06-10782
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / g. NH3 / ethanol / 24 h / 160 °C
2: 70 percent / hydrazine monohydrate / Pd/C / ethanol / 2.5 h / Heating
With
ammonia; hydrazine hydrate;
palladium on activated charcoal;
In
ethanol;
DOI:10.3987/COM-06-10782
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3.5 percent / KNO3; H2SO4 / 4 h / 0 - 10 °C
2: 53 percent / arsenic pentoxide; H2SO4 / 2 h / 150 °C
3: 98 percent / NH3 / ethanol / 22 h / 160 °C
4: 50 percent / H2 / Pd/C / ethanol / 3.5 h / 60 °C / 2280 Torr
With
arsenic(V) oxide; sulfuric acid; ammonia; hydrogen; potassium nitrate;
palladium on activated charcoal;
In
ethanol;
1: Nitration / 2: Cyclization / 3: Substitution / 4: Hydrogenolysis;
DOI:10.3987/COM-99-8766
