(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Base Information

Chemical Name:(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate
CAS No.:96481-74-2
Molecular Formula:C₂₄H₃₆O₃
Molecular Weight:372.548
Hs Code.:

Synonyms:(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Suppliers and Price of (10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Chemical Property:

Purity/Quality:

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Technology Process of (10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

There total 9 articles about (10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96481-69-5
(2S)-2-methyl-4-(benzyloxy)-1-butanal

: 96481-74-2
(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) H⁽¹⁺⁾ / 2.) toluene, 110 degC

With hydrogen cation;
DOI:10.1021/ja00296a040

Reference yield:

: 102745-43-7
(3S)-3-methyl-5-(benzyloxy)-1-pentene

: 96481-74-2
(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) O₃; 2.) zinc (dust), acetic acid / 1.) MeOH, -78 deg C, 30 min; 2.) 2 h, rt

2: 94 percent / Mg / tetrahydrofuran / reflux, 2h than rt., 90 min

3: propionic acid / toluene / 15 h / Heating

4: 96 percent / LiAlH₄ / diethyl ether / Ambient temperature

5: 80 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 15 h

6: 80.17 percent / 1.) Mg / tetrahydrofuran / Heating

7: propionic acid / toluene / Heating

With lithium aluminium tetrahydride; sodium acetate; ozone; magnesium; acetic acid; propionic acid; pyridinium chlorochromate; zinc; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja00275a055

Reference yield:

: 96481-77-5,102745-44-8,102745-45-9
(S)-1-Benzyloxy-3-methyl-5-methylene-heptan-4-ol

: 96481-74-2
(10S)-methyl 4,10-dimethyl-8-ethyl-12-(benzyloxy)dodeca-4(E),8(E)-dienoate

Guidance literature:: Multi-step reaction with 5 steps

1: propionic acid / toluene / 15 h / Heating

2: 96 percent / LiAlH₄ / diethyl ether / Ambient temperature

3: 80 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 15 h

4: 80.17 percent / 1.) Mg / tetrahydrofuran / Heating

5: propionic acid / toluene / Heating

With lithium aluminium tetrahydride; sodium acetate; magnesium; propionic acid; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja00275a055