2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

Base Information

Chemical Name:2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine
CAS No.:1033594-08-9
Molecular Formula:C₁₅H₁₉Cl₂N₃OSi
Molecular Weight:356.327
Hs Code.:

Synonyms:2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

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Chemical Property of 2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

Chemical Property:

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Technology Process of 2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

There total 1 articles about 2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-77-0
1,3,5-trichloro-2,4,6-triazine

: 65423-56-5
1-bromo-3-[(tert-butyldimethylsilyl)oxy]benzene

: 1033594-08-9
2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

Guidance literature:: 1-bromo-3-[(tert-butyldimethylsilyl)oxy]benzene; With magnesium; iodine; In tetrahydrofuran; at 20 ℃; for 2h; Heating / reflux;

1,3,5-trichloro-2,4,6-triazine; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

Reference yield: 86.0%

: 1033594-08-9
2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

: 62855-02-1
(R)-3-hydroxymethyl-1,2,3,4-tetrahydroisoquinoline

: 1033594-09-0
C₂₅H₃₁ClN₄O₂Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 1033594-08-9
2-[3-(tert-butyldimethylsilanyloxy)-phenyl]-4,6-dichloro-[1,3,5]triazine

: 1033594-06-7
3-[4-(hexahydropyrrolo[1,2-a]pyrazin-2-yl)-6-((3R)-hydroxymethyl-3,4-dihydro-1H-isoquinolin-2-yl)-[1,3,5]triazin-2-yl]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / -78 - 0 °C

3: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / Heating / reflux

With tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;