2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride

Base Information

• Chemical Name: 2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride
• CAS No.: 124318-74-7
• Molecular Formula: C₂₄H₁₆N₂O₄*ClH
• Molecular Weight: 432.863
• Mol file: 124318-74-7.mol

Synonyms:2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride

Chemical Property of 2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride

There total 1 articles about 2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2,9-bis(2,6-dimethoxyphenyl)-3-ethynyl-[1,10]-phenanthroline (124318-69-0) → 2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride (124318-74-7)

Guidance literature:

With pyridine hydrochloride; at 200 ℃; for 3h;

DOI:10.1002/1099-0690(200106)2001:11<2161::AID-EJOC2161>3.0.CO;2-2

Reference yield: 79.0%

2,9-Bis(2',6'-dihydroxyphenyl)-1,10-phenanthroline hydrochloride (124318-74-7) + bromopentene (1119-51-3) → 2,9-bis[2,6-bis(pent-4-enoxy)phenyl]-1,10-phenanthroline (356791-71-4)

Guidance literature:

With CsCO₃; In dimethyl sulfoxide; at 20 ℃; for 3h;

DOI:10.1002/1099-0690(200106)2001:11<2161::AID-EJOC2161>3.0.CO;2-2

upstream raw materials:

2,9-bis(2,6-dimethoxyphenyl)-3-ethynyl-[1,10]-phenanthroline

Downstream raw materials:

2,9-bis[2,6-bis(pent-4-enoxy)phenyl]-1,10-phenanthroline