3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

Base Information

Chemical Name:3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one
CAS No.:957211-53-9
Molecular Formula:C₂₄H₁₆F₇NO₅
Molecular Weight:531.384
Hs Code.:

Synonyms:3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

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Chemical Property of 3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

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Technology Process of 3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

There total 1 articles about 3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 957211-52-8
2-(3-nitro-3'-trifluoromethoxybiphenyl-2-ylmethyl)-3-oxo-3-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propionic acid ethyl ester

: 957211-53-9
3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

Guidance literature:: 2-(3-nitro-3'-trifluoromethoxybiphenyl-2-ylmethyl)-3-oxo-3-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propionic acid ethyl ester; With hydrogenchloride; acetic acid; for 9h;

With sodium hydroxide; In water; at 0 ℃;

Reference yield: 100.0%

: 957211-53-9
3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

: 957211-47-1
2-[3-(1,1,2,2-tetrafluoro-ethoxy)-phenyl]-5-(3-trifluoromethoxy-phenyl)-1,2,3,4-tetrahydro-quinoline

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 19h; under 2585.81 Torr; Product distribution / selectivity;

Reference yield: 86.0%

: 957211-53-9
3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one

: 957212-61-2
(αS)-3-nitro-α-[3-(1,1,2,2-tetrafluoroethoxy)-phenyl]-3'-(trifluoromethoxy)-[1,1'-biphenyl]-2-propanol

Guidance literature:: With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; toluene; at 20 ℃; for 0.25h;

3-(3-nitro-3'-trifluoromethoxybiphenyl-2-yl)-1-[3-(1,1,2,2-tetrafluoroethoxy)phenyl]propan-1-one; In tetrahydrofuran; toluene; at -25 - -10 ℃; for 3.5h;

With hydrogenchloride; methanol; In tetrahydrofuran; water; toluene;