C₃₄H₄₈B₂N₂OP₂

Base Information

Chemical Name:C₃₄H₄₈B₂N₂OP₂
CAS No.:1598430-65-9
Molecular Formula:C₃₄H₄₈B₂N₂OP₂
Molecular Weight:584.337
Hs Code.:

C<sub>34</sub>H<sub>48</sub>B<sub>2</sub>N<sub>2</sub>OP<sub>2</sub>

Synonyms:C₃₄H₄₈B₂N₂OP₂

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Chemical Property of C₃₄H₄₈B₂N₂OP₂

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Technology Process of C₃₄H₄₈B₂N₂OP₂

There total 4 articles about C₃₄H₄₈B₂N₂OP₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 685-83-6
bis(diethylamino)chlorophosphine

: 1598430-52-4
C₂₆H₂₅BBrOP

: 1598430-65-9
C₃₄H₄₈B₂N₂OP₂

Guidance literature:: C₂₆H₂₅BBrOP; With tert.-butyl lithium; In tetrahydrofuran; hexane; at -100 - -78 ℃; for 0.5h;

bis(diethylamino)chlorophosphine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 20.5h;

With dimethylsulfide borane complex; In tetrahydrofuran; hexane; for 2h;
DOI:10.1002/ejic.201301255

Reference yield:

: 1598430-52-4
C₂₆H₂₅BBrOP

: 1598430-65-9
C₃₄H₄₈B₂N₂OP₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / hexane; tetrahydrofuran / 0.67 h / -100 - -78 °C / Schlenk technique; Inert atmosphere

1.2: 20 h / -100 - 20 °C / Schlenk technique; Inert atmosphere

2.1: tetrahydrofuran / 2 h / Schlenk technique; Inert atmosphere

With tert.-butyl lithium; In tetrahydrofuran; hexane;
DOI:10.1002/ejic.201301255

Reference yield:

: C₂₆H₂₂BrOP

: 1598430-65-9
C₃₄H₄₈B₂N₂OP₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1 h / Schlenk technique; Inert atmosphere

2.1: tert.-butyl lithium / hexane; tetrahydrofuran / 0.67 h / -100 - -78 °C / Schlenk technique; Inert atmosphere

2.2: 20 h / -100 - 20 °C / Schlenk technique; Inert atmosphere

3.1: tetrahydrofuran / 2 h / Schlenk technique; Inert atmosphere

With tert.-butyl lithium; In tetrahydrofuran; hexane;
DOI:10.1002/ejic.201301255