Technology Process of Trihydro(dimethyl sulfide)boron
There total 20 articles about Trihydro(dimethyl sulfide)boron which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
dichloromethane;
B4H10:S(CH3)2 should kept close to stoich. value; soln. of B4H10 in CH2Cl2 placed in a Pyrex tube equipped with a Teflon valve, S(CH3)2 condensed into the tube at -197°C, warmed to -80°C, shaken; warmed to room temp., fractionated through -20 and -197°C traps under dynamic vac., -20°C trap Y-shaped, equipped with a Teflon valve on each of the upper arms, continuus pumped 5h;
- Guidance literature:
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B9H13S(CH3)2, Pyrolyse;
- Guidance literature:
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In
not given;
equimolar mixt. of products not sepd., detd. by (11)B-NMR spectroscopy;