dibromo-1,4 dimethoxy-2,3 naphtalene

Base Information

• Chemical Name: dibromo-1,4 dimethoxy-2,3 naphtalene
• CAS No.: 7311-17-3
• Molecular Formula: C₁₂H₁₀Br₂O₂
• Molecular Weight: 346.018

Synonyms:dibromo-1,4 dimethoxy-2,3 naphtalene

Chemical Property of dibromo-1,4 dimethoxy-2,3 naphtalene

Chemical Property:

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Technology Process of dibromo-1,4 dimethoxy-2,3 naphtalene

There total 1 articles about dibromo-1,4 dimethoxy-2,3 naphtalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2,3-dimethoxynaphthalene (10103-06-7) → dibromo-1,4 dimethoxy-2,3 naphtalene (7311-17-3) + 1-bromo-2,3-dimethoxynaphthalene (222555-02-4)

Guidance literature:

With aluminum tri-bromide; [bis(acetoxy)iodo]benzene; In acetonitrile; at 23 ℃;

DOI:10.1039/c8ra02982b

Reference yield:

dibromo-1,4 dimethoxy-2,3 naphtalene (7311-17-3) + o-fluorophenylboronic acid (1993-03-9) → 1-bromo-4-(2-fluorophenyl)-2,3-dimethoxynaphthalene

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 100 ℃; for 7h; Inert atmosphere;

upstream raw materials:

2,3-dimethoxynaphthalene

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