<<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

Base Information

Chemical Name:<<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane
CAS No.:116885-10-0
Molecular Formula:C₂₉H₂₂F₃N₂O₃P
Molecular Weight:534.474
Hs Code.:

Synonyms:<<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

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Technology Process of <<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

There total 2 articles about <<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 114610-23-0
ethyl 2-diazo-3-(2,4,5-trifluorophenyl)-3-oxopropionate

: 603-35-0
triphenylphosphine

: 116885-10-0
<<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

Guidance literature:: In di-isopropyl ether; for 3h; Ambient temperature;

Reference yield:

: 98349-24-7
ethyl 2,4,5-trifluorobenzoylacetate

: 116885-10-0
<<1-ethoxycarbonyl-2-(2,4,5-trifluorophenyl)-2-oxoethylidene>hydrazono>triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 90.4 percent / p-toluenesulfonyl azide, triethylamine / acetonitrile / 1.) 10 deg C, 15 min.; 2.) r.t., 2 h

2: 89 percent / diisopropyl ether / 3 h / Ambient temperature

With 4-toluenesulfonyl azide; triethylamine; In di-isopropyl ether; acetonitrile;