C₅₃H₅₄N₄O₃

Base Information

Chemical Name:C₅₃H₅₄N₄O₃
CAS No.:1428427-77-3
Molecular Formula:C₅₃H₅₄N₄O₃
Molecular Weight:795.037
Hs Code.:

C<sub>53</sub>H<sub>54</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₅₃H₅₄N₄O₃

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Chemical Property of C₅₃H₅₄N₄O₃

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Technology Process of C₅₃H₅₄N₄O₃

There total 19 articles about C₅₃H₅₄N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₅H₅₆N₄O₄

: 1428427-77-3
C₅₃H₅₄N₄O₃

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 ℃; for 3h;
DOI:10.1021/ol400469w

Reference yield:

: C₃₆H₄₃NO₃Si

: 1428427-77-3
C₅₃H₅₄N₄O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: copper(II) sulfate / toluene / 12 h / 20 °C / Inert atmosphere

5.1: tetrahydrofuran; chlorobenzene / 1 h / Inert atmosphere; Reflux

6.1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 24 h / Inert atmosphere

7.1: hydrogenchloride / 12 h / 20 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

8.2: 10 h / 20 °C / Inert atmosphere

9.1: sodium hydroxide / methanol; tetrahydrofuran; water / 3 h / 0 °C

With hydrogenchloride; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; Dess-Martin periodane; copper(II) sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; chlorobenzene; isopropyl alcohol; toluene; 5.1: |Grignard Reaction;
DOI:10.1021/ol400469w

Reference yield:

: C₃₀H₃₆N₂O₃

: 1428427-77-3
C₅₃H₅₄N₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

1.2: 10 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; tetrahydrofuran; water / 3 h / 0 °C

With triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol400469w