1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

Base Information

Chemical Name:1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride
CAS No.:644966-84-7
Molecular Formula:C₁₆H₂₃N₄O₄*Cl
Molecular Weight:370.836
Hs Code.:

Synonyms:1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

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Chemical Property of 1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

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Technology Process of 1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

There total 5 articles about 1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268679-79-3
C₁₄H₂₂N₄O₃

: 79-04-9
chloroacetyl chloride

: 644966-84-7
1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

Guidance literature:: C₁₄H₂₂N₄O₃; chloroacetyl chloride; In dichloromethane; at 0 ℃; for 1h;

With aluminum oxide; In methanol; dichloromethane; at 20 ℃; for 15h;

Reference yield:

: 1268679-81-7
C₁₆H₂₃ClN₄O₄

: 644966-84-7
1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

Guidance literature:: With aluminum oxide; In methanol; dichloromethane; at 20 ℃; for 15h;

Reference yield:

: 29968-78-3
2-(4-nitrophenyl)ethylamine monohydrochloride

: 644966-84-7
1,1-dimethyl-4-[2-(4-nitrophenethylamino)-2-oxoethyl]-3-oxopiperazinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropyl-carbodiimide; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: 1,4-dioxane / Microwave irradiation

3.1: dichloromethane / 1 h / 0 °C

3.2: 15 h / 20 °C

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In 1,4-dioxane; dichloromethane;