tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

Base Information

Chemical Name:tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate
CAS No.:1600526-59-7
Molecular Formula:C₂₈H₄₇NO₅
Molecular Weight:477.685
Hs Code.:

Synonyms:tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

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Chemical Property of tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

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Technology Process of tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

There total 8 articles about tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 19833-82-0
2-hydroxy-5-methoxy-3-tridecylcyclohexa-2,5-diene-1,4-dione

: 138007-25-7
4-(methylamino)butanoate t-butyl ester

: 1600526-59-7
tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

Guidance literature:: In ethanol; at 20 ℃; for 12h;

Reference yield:

: 4460-86-0,14374-62-0
asaraldehyde

: 1600526-59-7
tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: dihydrogen peroxide; sulfuric acid / methanol / 2 h / 20 °C / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 13 h / 20 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 2.08 h / -40 - 0 °C

3.2: 15 h / 0 - 20 °C / Inert atmosphere

4.1: ammonium cerium (IV) nitrate; water / acetonitrile / 3.5 h / -7 - 20 °C

5.1: ethanol / 12 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; ammonium cerium (IV) nitrate; sulfuric acid; water; dihydrogen peroxide; sodium hydride; In tetrahydrofuran; methanol; ethanol; hexane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 219144-65-7
1,2,4,5-tetramethoxy-3-tridecylbenzene

: 1600526-59-7
tert-butyl 4-((4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienyl)(methyl)amino)-butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium cerium (IV) nitrate; water / acetonitrile / 3.5 h / -7 - 20 °C

2: ethanol / 12 h / 20 °C

With ammonium cerium (IV) nitrate; water; In ethanol; acetonitrile;