2-(2-methoxyphenyl)-3-methylquinoxaline

Base Information

• Chemical Name: 2-(2-methoxyphenyl)-3-methylquinoxaline
• CAS No.: 74132-07-3
• Molecular Formula: C₁₆H₁₄N₂O
• Molecular Weight: 250.3

Synonyms:2-(2-methoxyphenyl)-3-methylquinoxaline

Chemical Property of 2-(2-methoxyphenyl)-3-methylquinoxaline

Chemical Property:

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Technology Process of 2-(2-methoxyphenyl)-3-methylquinoxaline

There total 2 articles about 2-(2-methoxyphenyl)-3-methylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

1-(2-methoxyphenyl)-2-nitropropene (6306-34-9) + 1,2-diamino-benzene (95-54-5) → 2-(2-methoxyphenyl)-3-methylquinoxaline (74132-07-3)

Guidance literature:

With copper(ll) bromide; In ethanol; at 110 ℃; for 4h; Green chemistry;

DOI:10.1016/j.tetlet.2012.11.127

Reference yield:

2-Bromo-2'-methoxypropiophenone (135333-25-4) + 1,2-diamino-benzene (95-54-5) → 2-(2-methoxyphenyl)-3-methylquinoxaline (74132-07-3)

Guidance literature:

With perchloric acid adsorbed on silica gel; In acetonitrile; at 20 ℃; for 5h;

DOI:10.1039/c4cc01327a

Reference yield: 89.0%

N,N-dimethyl acetamide (127-19-5,116057-81-9) + 2-(2-methoxyphenyl)-3-methylquinoxaline (74132-07-3) → 2-(4-methoxyphenyl)-3-vinylquinoxaline (1415584-10-9)

Guidance literature:

With dipotassium peroxodisulfate; iron(III) chloride hexahydrate; at 110 ℃; for 3h; Sealed tube;

DOI:10.1039/c2cc36708d

upstream raw materials:

1-(2-methoxyphenyl)-2-nitropropene

1,2-diamino-benzene

2-Bromo-2'-methoxypropiophenone

Downstream raw materials:

2-(4-methoxyphenyl)-3-vinylquinoxaline

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