tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

Base Information

Chemical Name:tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide
CAS No.:1341126-81-5
Molecular Formula:C₁₇H₂₃N₅O₄S
Molecular Weight:393.467
Hs Code.:

Synonyms:tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

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Chemical Property of tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

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Technology Process of tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

There total 4 articles about tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1341126-80-4
tert-butyl 5-(prop-2-yn-1-yl)-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

: 622-79-7
benzyl azide

: 1341126-81-5
tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

Guidance literature:: With sodium ascorbate; copper(II) sulfate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1016/j.bmc.2011.08.054

Reference yield:

: 147000-89-3
N-tert-butyloxycarbonylsulfamoyl chloride

: 1341126-81-5
tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 - 20 °C

2.1: potassium carbonate / dimethyl sulfoxide / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h

3.2: 20 °C

4.1: sodium ascorbate; copper(II) sulfate / water; tert-butyl alcohol / 20 °C

With sodium ascorbate; sodium hydride; potassium carbonate; copper(II) sulfate; triethylamine; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2011.08.054

Reference yield:

: 263719-76-2
tert-butyl 1,2,5-thiadiazolidine-2-carboxylate1,1-dioxide

: 1341126-81-5
tert-butyl 5-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1,2,5-thiadiazolidine-2-carboxylate 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h

1.2: 20 °C

2.1: sodium ascorbate; copper(II) sulfate / water; tert-butyl alcohol / 20 °C

With sodium ascorbate; sodium hydride; copper(II) sulfate; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2011.08.054