3-AMINO-5-[1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE]-2-THIOXO-THIAZOLIDIN-4-ONE

Base Information

• Chemical Name: 3-AMINO-5-[1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE]-2-THIOXO-THIAZOLIDIN-4-ONE
• CAS No.: 35533-27-8
• Molecular Formula: C12H13 N3 O S2
• Molecular Weight: 279.38112
• Hs Code.: 2934999090
• Mol file: 35533-27-8.mol

Synonyms:Rhodanine,3-amino-5-(p-dimethylaminobenzylidene)- (6CI); 5-(4-Dimethylaminobenzylidene)-3-amino-4-oxo-2-thioxothiazolidine

Chemical Property of 3-AMINO-5-[1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE]-2-THIOXO-THIAZOLIDIN-4-ONE

Chemical Property:

• Boiling Point: 462.9±55.0 °C(Predicted)
• PKA: 3.72±0.24(Predicted)
• PSA: 106.96000
• Density: 1.42±0.1 g/cm3(Predicted)
• LogP: 2.46570

Purity/Quality:

3-AMINO-5-(1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE)-2-THIOXO-THIAZOLIDIN-4-ONE 95.00% ^*data from reagent suppliers

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Technology Process of 3-AMINO-5-[1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE]-2-THIOXO-THIAZOLIDIN-4-ONE

There total 4 articles about 3-AMINO-5-[1-(4-DIMETHYLAMINO-PHENYL)-METH-(Z)-YLIDENE]-2-THIOXO-THIAZOLIDIN-4-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

3-aminorhodanine (1438-16-0) + 4-dimethylamino-benzaldehyde (100-10-7) → 3-Amino-5-(4-dimethylaminobenzyliden)rhodanin (35533-27-8)

Guidance literature:

With sodium acetate; In methanol; for 0.416667h; Heating;

DOI:10.1021/jm050859x

Reference yield:

3-aminorhodanine (1438-16-0) + 4-dimethylamino-benzaldehyde (100-10-7) → 3-amino-5-(p-dimethylamino)benzylidenethiazolidine-2-thion-4-one (35533-27-8)

Guidance literature:

With ammonia; ammonium chloride;

Reference yield:

3-(4-dimethylamino-benzylidenamino)-2-thioxo-thiazolidin-4-one (19745-77-8) + aniline (62-53-3) → 3-amino-5-(p-dimethylamino)benzylidenethiazolidine-2-thion-4-one (35533-27-8)

Guidance literature:

With ethanol;

upstream raw materials:

3-aminorhodanine

4-dimethylamino-benzaldehyde

3-(4-dimethylamino-benzylidenamino)-2-thioxo-thiazolidin-4-one

aniline

Downstream raw materials:

3-formamido-5-(p-dimethylamino)benzylidenethiazolidine-2-thion-4-one

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