4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane

Base Information

• Chemical Name: 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane
• CAS No.: 127936-42-9
• Molecular Formula: C₂₂H₂₈NO₄P
• Molecular Weight: 401.442
• Mol file: 127936-42-9.mol

Synonyms:4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane

Chemical Property of 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane

There total 2 articles about 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-hydro-4,5-dimethyl-2-oxo-1,3,2-dioxaphospholane (16352-17-3,26349-89-3,26349-90-6,26349-91-7) + (Z)-1-(1,2-diphenylvinyl)morpholine (4176-68-5) → 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane (127936-42-9)

Guidance literature:

In benzene; at 80 ℃; for 5h;

Reference yield:

1,2-dimethylethylene hydrogen phosphite (3441-13-2) + 1-morpholino-1,2-diphenylethene (18239-50-4) → 4,5-dimethyl-2-(1-morpholino-1,2-diphenylethyl)-2-oxo-1,3,2-dioxaphospholane (127936-42-9)

Guidance literature:

at 80 ℃; for 5h;

upstream raw materials:

1,2-dimethylethylene hydrogen phosphite

1-morpholino-1,2-diphenylethene

2-hydro-4,5-dimethyl-2-oxo-1,3,2-dioxaphospholane

(Z)-1-(1,2-diphenylvinyl)morpholine