N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

Base Information

Chemical Name:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide
CAS No.:1260172-46-0
Molecular Formula:C₂₇H₂₀Br₂FN₃O₄S
Molecular Weight:661.346
Hs Code.:

Synonyms:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

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Chemical Property of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

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Technology Process of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

There total 4 articles about N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1286272-06-7
C₂₇H₂₁Br₂N₃O₅S

: 1260172-46-0
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja108211m

Reference yield:

: 6825-20-3
3,6-dibromo-9H-carbazole

: 1260172-46-0
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 20 °C

2.1: n-butyllithium / hexane; toluene / 0.17 h / -78 °C / Inert atmosphere

2.2: 20 - 100 °C / Inert atmosphere

3.1: diethylamino-sulfur trifluoride / dichloromethane / -78 - 20 °C / Inert atmosphere

With n-butyllithium; diethylamino-sulfur trifluoride; potassium hydroxide; In hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja108211m

Reference yield:

: 1576-44-9
N-nosylaniline

: 1260172-46-0
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-fluoropropyl)-4-nitro-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; toluene / 0.17 h / -78 °C / Inert atmosphere

1.2: 20 - 100 °C / Inert atmosphere

2.1: diethylamino-sulfur trifluoride / dichloromethane / -78 - 20 °C / Inert atmosphere

With n-butyllithium; diethylamino-sulfur trifluoride; In hexane; dichloromethane; toluene;
DOI:10.1021/ja108211m