CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4

Base Information

• Chemical Name: CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4
• CAS No.: 208589-81-5
• Molecular Formula: C₁₉H₂₉N₂OPd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1271.09

Synonyms:CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4

Chemical Property of CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4

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Technology Process of CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4

There total 2 articles about CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)=CH₃C₆H₄CHCH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2B[C₆H₃(CF₃)2]4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[((CH3)2CHNCH)2PdCOCHC6H4CH3CH2COCH3CO](1+)*[B(C6H3(CF3)2)4](1-)=[((CH3)2CHNCH)2PdCOCHC6H4CH3CH2COCH3CO][B(C6H3(CF3)2)4] (350017-08-2) → CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 (208589-81-5)

Guidance literature:

With nitrogen; In not given; (N2); bubbling N2 through a soln. of palladium complex at -50°C for 4 min;

DOI:10.1021/om000971n

Reference yield: 100.0%

1-ethenyl-4-methylbenzene (622-97-9,24936-41-2) + [Pd(CH3)(carbonyl)(1,4-diisopropyl-1,4-diaza-1,3-butadiene)](1+)[B(3,5-(CF3)2C6H3)4](1-) (208589-78-0) → CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 (208589-81-5)

Guidance literature:

In chloroform-d1; addn. of p-methylstyrene to complex soln. at -10°C, gentle heating to 20°C;

DOI:10.1039/a801158c

Reference yield:

CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3C6H4CHCH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 (208589-81-5) + carbon monoxide (201230-82-2) → CH3C6H4CH(CO)CH2COCH3Pd(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-) (208589-83-7)

Guidance literature:

In chloroform; at -10°C for 15 min;

DOI:10.1039/a801158c

upstream raw materials:

1-ethenyl-4-methylbenzene

[Pd(CH₃)(carbonyl)(1,4-diisopropyl-1,4-diaza-1,3-butadiene)]⁽¹⁺⁾[B(3,5-(CF₃)2C₆H₃)4]^(1-)

[((CH₃)2CHNCH)2PdCOCHC₆H₄CH₃CH₂COCH₃CO]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[((CH₃)2CHNCH)2PdCOCHC₆H₄CH₃CH₂COCH₃CO][B(C₆H₃(CF₃)2)4]

Downstream raw materials:

CH₃C₆H₄CH(CO)CH₂COCH₃Pd(CH₃)2CHNCHCHNCH(CH₃)2⁽¹⁺⁾*B[C₆H₃(CF₃)2]4^(1-)

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