<α,α-(2)H2>benzyl phenylmethanethiosulphinate

Base Information

Chemical Name:<α,α-(2)H2>benzyl phenylmethanethiosulphinate
CAS No.:73975-39-0
Molecular Formula:C₁₄H₁₄OS₂
Molecular Weight:264.381
Hs Code.:

Synonyms:<α,α-(2)H2>benzyl phenylmethanethiosulphinate

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Chemical Property of <α,α-(2)H2>benzyl phenylmethanethiosulphinate

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Technology Process of <α,α-(2)H2>benzyl phenylmethanethiosulphinate

There total 5 articles about <α,α-(2)H2>benzyl phenylmethanethiosulphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 41719-05-5
phenylmethanesulfinyl chloride

: 73975-41-4
<α,α-(2)H2>toluene-α-thiol

: 73975-39-0
<α,α-(2)H2>benzyl phenylmethanethiosulphinate

Guidance literature:: With triethylamine; In diethyl ether; at -20 ℃; for 0.333333h;
DOI:10.1039/P29800000432

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 73975-39-0
<α,α-(2)H2>benzyl phenylmethanethiosulphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / LiAlD₄ / diethyl ether

2: 75 percent / thiourea / aq. HBr / 9 h / Heating

3: 56 percent / triethylamine / diethyl ether / 0.33 h / -20 °C

With lithium aluminium deuteride; triethylamine; thiourea; In diethyl ether; hydrogen bromide;
DOI:10.1039/P29800000432

Reference yield:

: 150-60-7
dibenzyl disulphide

: 73975-39-0
<α,α-(2)H2>benzyl phenylmethanethiosulphinate

Guidance literature:: Multi-step reaction with 2 steps

1: chlorine / acetic anhydride / -10 °C

2: 56 percent / triethylamine / diethyl ether / 0.33 h / -20 °C

With chlorine; triethylamine; In diethyl ether; acetic anhydride;
DOI:10.1039/P29800000432