4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

Base Information

Chemical Name:4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one
CAS No.:145887-34-9
Molecular Formula:C₂₅H₂₃N₅O₂
Molecular Weight:425.49
Hs Code.:

Synonyms:4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

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Chemical Property of 4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

Chemical Property:

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Technology Process of 4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

There total 5 articles about 4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 145887-41-8
(+/-)-1-(4-methoxyphenyl)-4-(tetrazol-5-ylmethyl)azetidin-2-one

: 908093-98-1
diazodiphenylmethane

: 145887-34-9
4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

: 145887-53-2
4-<1-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

Guidance literature:: In 1,4-dioxane; for 168h; Ambient temperature;
DOI:10.1039/P19920003061

Reference yield:

: 145985-24-6
4-hydroxymethyl-1-(4-methoxyphenyl)-2-azetidinone

: 145887-34-9
4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / pyridine / 3 h / Ambient temperature

2: 89 percent / sodium iodide / acetone / 12 h / Heating

3: 62 percent / dimethylformamide / 6 h / Ambient temperature

4: 82 percent / sodium azide, AlCl₃ / tetrahydrofuran / 24 h / Heating

5: 79 percent / dioxane / 168 h / Ambient temperature

With pyridine; aluminium trichloride; sodium azide; sodium iodide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; acetone;
DOI:10.1039/P19920003061

Reference yield:

: 145887-49-6
rac-4-iodomethyl-1-(4-methoxyphenyl)-4-oxoazetidin-2-one

: 145887-34-9
4-<2-(diphenylmethyl)tetrazol-5-ylmethyl>-1-(4-methoxyphenyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / dimethylformamide / 6 h / Ambient temperature

2: 82 percent / sodium azide, AlCl₃ / tetrahydrofuran / 24 h / Heating

3: 79 percent / dioxane / 168 h / Ambient temperature

With aluminium trichloride; sodium azide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/P19920003061