N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide

Base Information

• Chemical Name: N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide
• CAS No.: 135190-65-7
• Molecular Formula: C₁₇H₂₄INO
• Molecular Weight: 385.288
• Mol file: 135190-65-7.mol

Synonyms:N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide

Chemical Property of N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide

There total 1 articles about N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-iodophenyl)-3,7-dimethyloct-6-enamide + methyl iodide (74-88-4) → N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide (135190-65-7)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1.) DMSO, 0 deg C, 2 h, 2.) DMSO, 4.5 h;

DOI:10.1016/S0040-4020(01)90466-1

Reference yield: 84.0%

N-(o-iodophenyl)-N-methyl-3,7-dimethyl-6-octenamide (135190-65-7) → N-methyl-N-phenyl-5-isopropyl-2-methylcyclopentanecarboxamide (135190-84-0,135269-15-7)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃;

DOI:10.1021/jo00014a001

upstream raw materials:

methyl iodide

Downstream raw materials:

N-methyl-N-phenyl-5-isopropyl-2-methylcyclopentanecarboxamide