3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate

Base Information

• Chemical Name: 3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate
• CAS No.: 900809-23-6
• Molecular Formula: C₂₉H₃₂FN₃O₅S₂
• Molecular Weight: 585.721

Synonyms:3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate

Chemical Property of 3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate

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Technology Process of 3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate

There total 1 articles about 3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl]-N-(2-(R,S)-fluoro-3-hydroxypropyl)-4-methylbenzamide (900809-22-5) + methanesulfonyl chloride (124-63-0) → 3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate (900809-23-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

3-[[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl](4-methylbenzoyl)amino]-2-(R,S)-fluoropropyl methanesulfonate (900809-23-6) → N-(3-azido-2-(R,S)-fluoropropyl)-N-[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl]-4-methylbenzamide (900809-24-7)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 60 ℃;

upstream raw materials:

N-[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl]-N-(2-(R,S)-fluoro-3-hydroxypropyl)-4-methylbenzamide

methanesulfonyl chloride

Downstream raw materials:

N-(3-azido-2-(R,S)-fluoropropyl)-N-[1-(3-benzyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidin-2-yl)-2-(R,S)-methylpropyl]-4-methylbenzamide

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