1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide

Base Information

• Chemical Name: 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide
• CAS No.: 115094-74-1
• Molecular Formula: C₂₇H₃₃N₂S₂*I
• Molecular Weight: 576.609

Synonyms:1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide

Chemical Property of 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide

Chemical Property:

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Technology Process of 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide

There total 4 articles about 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-dibenzyl-1,3-diaminopropane (10239-34-6) → 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide (115094-74-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / dimethylformamide / 1 h / Heating

2: 86 percent / 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide / 1,2-dimethoxy-ethane

3: acetone

With 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo00005a043

Reference yield:

2--5,5-dimethylcyclohexane-1,3-dione → 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide (115094-74-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / dimethylformamide / 1 h / Heating

2: 86 percent / 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide / 1,2-dimethoxy-ethane

3: acetone

With 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo00005a043

Reference yield:

1,3-Dibenzyl-2-(4,4-dimethyl-2,6-dioxocyclohexylidene)hexahydropyrimidine (132206-16-7) → 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-3,4,5,6-tetrahydro-pyrimidin-1-ium; iodide (115094-74-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide / 1,2-dimethoxy-ethane

2: acetone

With 2,4-bis<4-(methylthio)phenyl>-1,3,2,4-dithiadiphosphetane 2,4-disulfide; In 1,2-dimethoxyethane; acetone;

DOI:10.1021/jo00005a043

upstream raw materials:

1,3-Dibenzyl-2-(4,4-dimethyl-2,6-dithioxocyclohexylidene)hexahydropyrimidine

methyl iodide

N,N'-dibenzyl-1,3-diaminopropane

1,3-Dibenzyl-2-(4,4-dimethyl-2,6-dioxocyclohexylidene)hexahydropyrimidine

Downstream raw materials:

C₃₃H₃₈N₂O₄S₂

Dimethyl 4--amino>-5-(methylthio)-7H-7,7-dimethylbenzothiopyran-2,3-dicarboxylate

4-(Benzyl-{3-[benzyl-((E)-1,2-bis-methoxycarbonyl-vinyl)-amino]-propyl}-amino)-7,7-dimethyl-5-methylsulfanyl-7H-thiochromene-2,3-dicarboxylic acid dimethyl ester

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