-(+)-4-chloro-1-phenyl-3-buten-1-ol

Base Information

Chemical Name:-(+)-4-chloro-1-phenyl-3-buten-1-ol
CAS No.:90760-65-9
Molecular Formula:C₁₀H₁₁ClO
Molecular Weight:182.65
Hs Code.:

<R-(Z)>-(+)-4-chloro-1-phenyl-3-buten-1-ol

Synonyms:-(+)-4-chloro-1-phenyl-3-buten-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -(+)-4-chloro-1-phenyl-3-buten-1-ol

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Technology Process of -(+)-4-chloro-1-phenyl-3-buten-1-ol

There total 5 articles about -(+)-4-chloro-1-phenyl-3-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 158813-39-9
2-(Z-3-chloroprop-2-enyl)-4,4,5,5-tetramethyl-1,2,3-dioxaborolane

: 100-52-7
benzaldehyde

: 90760-65-9
-(+)-4-chloro-1-phenyl-3-buten-1-ol

Guidance literature:: With methanol; (2S)-2-((2-hydroxy-3-(triphenylsilyl)benzyl)amino)-2-(3-hydroxyadamantan-1-yl) 1-(isoindolin-2-yl)ethan-1-one; zinc dimethoxide; In toluene; at 22 ℃; for 14h; stereoselective reaction; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.9b11178

Reference yield:

: 158813-39-9
2-(Z-3-chloroprop-2-enyl)-4,4,5,5-tetramethyl-1,2,3-dioxaborolane

: 100-52-7
benzaldehyde

: 90760-65-9
-(+)-4-chloro-1-phenyl-3-buten-1-ol

: -4-chloro-1-phenyl-3-buten-1-ol

Guidance literature:: With methanol; C₃₃H₃₈N₂O₂Si; zinc dimethoxide; In toluene; at 22 ℃; for 14h; Reagent/catalyst; Overall yield = 94 percent; stereoselective reaction; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.9b11178

Reference yield:

: 158813-39-9
2-(Z-3-chloroprop-2-enyl)-4,4,5,5-tetramethyl-1,2,3-dioxaborolane

: 100-52-7
benzaldehyde

: 88086-64-0
2-chloro-1-phenylbut-3-en-1-ol

: 90760-65-9
-(+)-4-chloro-1-phenyl-3-buten-1-ol

: -4-chloro-1-phenyl-3-buten-1-ol

Guidance literature:: With methanol; (S)-2-((2-hydroxy-3-(triphenylsilyl)benzyl)amino)-N,N,3-trimethylbutanamide; zinc dimethoxide; In toluene; at 22 ℃; for 14h; Overall yield = 79 percent; stereoselective reaction; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.9b11178