2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine

Base Information

• Chemical Name: 2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine
• CAS No.: 78304-65-1
• Molecular Formula: C₁₁H₁₅N₂OPS₂
• Molecular Weight: 286.359
• Mol file: 78304-65-1.mol

Synonyms:2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine

Chemical Property of 2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine

There total 1 articles about 2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-(dimethylamino)-3-phenyl-1,3,2-oxazaphospholidine (32018-62-5) + carbon disulfide (75-15-0,12122-00-8) → 2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine (78304-65-1)

Guidance literature:

In diethyl ether;

Reference yield: 87.0%

2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine (78304-65-1) + diethylamine (109-89-7) → diethylammonium diethyldithiocarbamate (1518-58-7) + N,N-diethyl-3-phenyl-1,3,2-oxazaphospholidin-2-amine (31707-09-2)

Guidance literature:

Reference yield: 86.0%

2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine (78304-65-1) → 2-(dimethylamino)-3-phenyl-1,3,2-oxazaphospholidine 2-sulfide (51729-74-9)

Guidance literature:

With sulfur; In benzene; at 80 ℃; for 1.16667h;

upstream raw materials:

2-(dimethylamino)-3-phenyl-1,3,2-oxazaphospholidine

carbon disulfide

Downstream raw materials:

2-ethoxy-3-phenyl-1,3,2-oxazaphospholidine

2-(dimethylamino)-3-phenyl-1,3,2-oxazaphospholidine 2-sulfide

2-(dimethylthiocarbamoylthio)-3-phenyl-1,3,2-oxazaphospholidine 2-sulfide

diethylammonium diethyldithiocarbamate