C₃₄H₄₆N₄O₃S₂

Base Information

Chemical Name:C₃₄H₄₆N₄O₃S₂
CAS No.:1393910-25-2
Molecular Formula:C₃₄H₄₆N₄O₃S₂
Molecular Weight:622.896
Hs Code.:

C<sub>34</sub>H<sub>46</sub>N<sub>4</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:C₃₄H₄₆N₄O₃S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₆N₄O₃S₂

Chemical Property:

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Technology Process of C₃₄H₄₆N₄O₃S₂

There total 14 articles about C₃₄H₄₆N₄O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393910-24-1
C₃₄H₄₄N₄O₅S₂

: 1393910-25-2
C₃₄H₄₆N₄O₃S₂

Guidance literature:: With methanol; tin(II) chloride dihdyrate; at 65 ℃; Reflux;

Reference yield:

: 53815-60-4
1-(2-chloroethoxy)-2-methoxybenzene

: 1393910-25-2
C₃₄H₄₆N₄O₃S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogenchloride / water; 1,4-dioxane / 2 h / Cooling with ice

2.1: sodium acetate / 2 h / Reflux

3.1: ammonia / methanol / 15 h

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice

4.2: 0.17 h / -78 °C

5.1: sodium ethanolate / ethanol / 16 h / 0 - 20 °C / Cooling with ice

6.1: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 6 h / 27 °C

7.1: thionyl chloride; N,N-dimethyl-formamide / benzene / 20 °C / Inert atmosphere

7.2: 0 °C

8.1: diisobutylaluminium hydride / dichloromethane / 0.75 h / -78 °C

8.2: 12 h / 27 °C

9.1: potassium carbonate / 1 h / 120 °C

10.1: tin(II) chloride dihdyrate / methanol / 5 h / 65 °C

With hydrogenchloride; thionyl chloride; oxalyl dichloride; tin(II) chloride dihdyrate; lithium hydroxide monohydrate; ammonia; sodium ethanolate; sodium acetate; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; benzene;

Reference yield:

: 348618-22-4
2-[(acetyloxy)methyl]-4-(2-chloroethoxy)-5-methoxybenzyl acetate

: 1393910-25-2
C₃₄H₄₆N₄O₃S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: ammonia / methanol / 15 h

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice

2.2: 0.17 h / -78 °C

3.1: sodium ethanolate / ethanol / 16 h / 0 - 20 °C / Cooling with ice

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 6 h / 27 °C

5.1: thionyl chloride; N,N-dimethyl-formamide / benzene / 20 °C / Inert atmosphere

5.2: 0 °C

6.1: diisobutylaluminium hydride / dichloromethane / 0.75 h / -78 °C

6.2: 12 h / 27 °C

7.1: potassium carbonate / 1 h / 120 °C

8.1: tin(II) chloride dihdyrate / methanol / 5 h / 65 °C

With thionyl chloride; oxalyl dichloride; tin(II) chloride dihdyrate; lithium hydroxide monohydrate; ammonia; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; dimethyl sulfoxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; benzene;