Technology Process of (4-chloro-1,1-dimethoxybutyl)benzene
There total 1 articles about (4-chloro-1,1-dimethoxybutyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Montmorillonite K10 clay;
for 72h;
Inert atmosphere;
DOI:10.1021/ja8045475
- Guidance literature:
-
(4-chloro-1,1-dimethoxybutyl)benzene;
With
naphthalene; Lithium-high sodium;
In
tetrahydrofuran;
at -78 ℃;
for 2h;
Inert atmosphere;
4-methoxypent-3-en-2-one;
In
tetrahydrofuran;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ja8045475
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; Diethyl 2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate; α-aminoacrylic acid;
In
N,N-dimethyl acetamide;
for 18h;
Irradiation;
Sealed tube;
Inert atmosphere;
DOI:10.1021/acs.orglett.9b02273
