N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide

Base Information

• Chemical Name: N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide
• CAS No.: 1398805-45-2
• Molecular Formula: C₂₄H₂₆NO₃P
• Molecular Weight: 407.449

Synonyms:N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide

Chemical Property of N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide

Chemical Property:

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Technology Process of N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide

There total 1 articles about N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

benzaldehyde (100-52-7) + phenylphosphonic acid ethyl ester N,N-diethylamide → N,N-diethyl-3-phenyl-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide + N,N-diethyl-3-phenyl-3-(hydroxy(phenyl)methyl)-1,3-dihydro-2,1-benzoxaphosphol-1-amine 1-oxide (1398805-45-2)

Guidance literature:

phenylphosphonic acid ethyl ester N,N-diethylamide; With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 0.416667h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; at -78 - 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/jo301526k

upstream raw materials:

benzaldehyde

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