(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Base Information

Chemical Name:(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)
CAS No.:352665-20-4
Molecular Formula:C₂₅H₂₇N₅O₄
Molecular Weight:461.52
Hs Code.:

Synonyms:(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Suppliers and Price of (S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

There total 5 articles about (S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 593-56-6
N-methoxylamine hydrochloride

: 352665-13-5
(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide

: 352665-20-4
(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Guidance literature:: With pyridine; In methanol; at 50 ℃; for 1.5h;
DOI:10.1021/ja010066+

Reference yield:

: 118-48-9
isatoic anhydride

: 352665-20-4
(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Guidance literature:: Multi-step reaction with 4 steps

1: 9.8 g / benzene / 5 h / Heating

2: 87 percent / Me₃Al / CH₂Cl₂; toluene / 18 h / 20 °C

3: 81 percent / NaHCO₃ / ethyl acetate; H₂O / 0 - 20 °C

4: 1.39 g / pyridine / methanol / 1.5 h / 50 °C

With pyridine; trimethylaluminum; sodium hydrogencarbonate; In methanol; dichloromethane; water; ethyl acetate; toluene; benzene;
DOI:10.1021/ja010066+

Reference yield:

: 85612-29-9
N_b-(2-aminobenzoyl)-L-tryptophan methyl ester

: 352665-20-4
(S)-N-allyl-α-(o-pyruvamidobenzamido)indole-3-propionamide, 2-(E)-(O-benzyloxime)

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / Me₃Al / CH₂Cl₂; toluene / 18 h / 20 °C

2: 81 percent / NaHCO₃ / ethyl acetate; H₂O / 0 - 20 °C

3: 1.39 g / pyridine / methanol / 1.5 h / 50 °C

With pyridine; trimethylaluminum; sodium hydrogencarbonate; In methanol; dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/ja010066+