C₃₉H₆₇NO₈Si₂

Base Information

Chemical Name:C₃₉H₆₇NO₈Si₂
CAS No.:1611465-59-8
Molecular Formula:C₃₉H₆₇NO₈Si₂
Molecular Weight:734.134
Hs Code.:

C<sub>39</sub>H<sub>67</sub>NO<sub>8</sub>Si<sub>2</sub>

Synonyms:C₃₉H₆₇NO₈Si₂

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Chemical Property of C₃₉H₆₇NO₈Si₂

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Technology Process of C₃₉H₆₇NO₈Si₂

There total 2 articles about C₃₉H₆₇NO₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₃₃H₅₃NO₈Si

: 1611465-59-8
C₃₉H₆₇NO₈Si₂

Guidance literature:: With 1H-imidazole; triethylsilyl chloride; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201304776

Reference yield: 86.0%

: 994-30-9
triethylsilyl chloride

: C₃₃H₅₃NO₈Si

: 1611465-59-8
C₃₉H₆₇NO₈Si₂

: C₃₉H₆₇NO₈Si₂

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/acs.joc.6b00489

Reference yield:

: 1611465-59-8
C₃₉H₆₇NO₈Si₂

: C₄₅H₅₆O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 - 0 °C / Inert atmosphere

1.2: 6 h / 0 °C / Inert atmosphere

2.1: triethylsilane; palladium 10% on activated carbon / dichloromethane / 16 h / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.25 h / -78 °C / Inert atmosphere

3.2: 0.75 h / -78 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / n-heptane; methanol; toluene / 1.75 h / -78 - 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

With triethylsilane; n-butyllithium; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; tert.-butyl lithium; diisobutylaluminium hydride; In tetrahydrofuran; methanol; hexane; n-heptane; dichloromethane; toluene; pentane;
DOI:10.1002/chem.201304776