isopropyl 2-cyano-3-phenylacrylate

Base Information

Chemical Name:isopropyl 2-cyano-3-phenylacrylate
CAS No.:18300-86-2
Molecular Formula:C₁₃H₁₃NO₂
Molecular Weight:215.252
Hs Code.:

Synonyms:isopropyl 2-cyano-3-phenylacrylate

Suppliers and Price of isopropyl 2-cyano-3-phenylacrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl 2-cyano-3-phenylacrylate

Chemical Property:

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Technology Process of isopropyl 2-cyano-3-phenylacrylate

There total 2 articles about isopropyl 2-cyano-3-phenylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100-52-7
benzaldehyde

: 67-63-0,8013-70-5
isopropyl alcohol

: 107-91-5
cyanoacetic acid amide

: 18300-86-2
isopropyl 2-cyano-3-phenylacrylate

Guidance literature:: With 1,3,5-trichloro-2,4,6-triazine; In neat (no solvent); at 80 ℃; for 12h;
DOI:10.1002/cjoc.201500420

Reference yield:

: 13361-30-3
isopropyl cyanoacetate

: 100-52-7
benzaldehyde

: 18300-86-2
isopropyl 2-cyano-3-phenylacrylate

Guidance literature:: With Er(1,3,5-benzenetricarboxylate)(1,2-ethanediamine)0.75(H₂O)0.25; In cyclohexane; at 40 ℃; for 2h; Catalytic behavior;
DOI:10.1016/S1872-2067(15)60945-7

Reference yield: 81.0%

: 80466-34-8,4488-48-6
2,4-hexadienal

: 18300-86-2
isopropyl 2-cyano-3-phenylacrylate

: C₁₉H₂₁NO₃

: C₁₉H₂₁NO₃

: 1279108-78-9
C₁₉H₂₁NO₃

Guidance literature:: With 4-Fluorobenzoic acid; C₄₁H₆₉NO₃Si; In chloroform; at 50 ℃; for 60h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja1112194