cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Base Information

Chemical Name:cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene
CAS No.:934389-61-4
Molecular Formula:C₂₆H₂₈N₂O₄S₂
Molecular Weight:496.651
Hs Code.:

Synonyms:cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

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Technology Process of cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

There total 3 articles about cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 934389-54-5
cis-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

: 106-96-7
propargyl bromide

: 934389-61-4
cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.092

Reference yield:

: 102312-67-4,105249-35-2,108796-57-2,118157-55-4
cis-cyclohex-3-enyl-1,2-diamine dihydrochloride

: 934389-61-4
cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂

2: 96 percent / NaH / dimethylformamide

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.092

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 934389-61-4
cis-N,N'-bis-(prop-2-ynyl)-N,N'-bis-(p-toluenesulfonyl)-1,2-diaminocyclohex-4-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂

2: 96 percent / NaH / dimethylformamide

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.092