2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide

Base Information

Chemical Name:2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide
CAS No.:78466-25-8
Molecular Formula:C₉H₈Cl₂N₂O₃
Molecular Weight:263.08
Hs Code.:
UNII:Z77W9CT56Y

Synonyms:2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide;78466-25-8;Z77W9CT56Y;Acetanilide, 2,2-dichloro-N-methyl-4'-nitro-;Acetamide, 2,2-dichloro-N-methyl-N-(4-nitrophenyl)-

Suppliers and Price of 2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:261.9911975
Heavy Atom Count:16
Complexity:272

Purity/Quality:: 95%+HPLC ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C1=CC=C(C=C1)[N+](=O)[O-])C(=O)C(Cl)Cl

Technology Process of 2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide

There total 3 articles about 2,2-Dichloro-N-methyl-N-(4-nitrophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 126434-07-9
N-methyl-4-nitrotrichloroacetanilide

: 78466-25-8
p-nitro-N-methyldichloroacetanilide

Guidance literature:: With sodium trichloroacetate; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃;

Reference yield:

: 36558-96-0
N-methyl-N-phenyltrichloroacetamide

: 78466-25-8
p-nitro-N-methyldichloroacetanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / acetic anhydride, potassium nitrate, conc. sulfuric acid / acetic acid / 2 h

2: 70 percent / sodium trichloroacetate / benzyltriethylammonium chloride / CHCl₃ / 60 °C

With sulfuric acid; sodium trichloroacetate; acetic anhydride; potassium nitrate; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; acetic acid;

Reference yield:

: 100-61-8
N-methylaniline

: 78466-25-8
p-nitro-N-methyldichloroacetanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / pyridine / benzene

2: 40 percent / acetic anhydride, potassium nitrate, conc. sulfuric acid / acetic acid / 2 h

3: 70 percent / sodium trichloroacetate / benzyltriethylammonium chloride / CHCl₃ / 60 °C

With pyridine; sulfuric acid; sodium trichloroacetate; acetic anhydride; potassium nitrate; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; acetic acid; benzene;