(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

Base Information

Chemical Name:(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine
CAS No.:1123309-26-1
Molecular Formula:C₂₄H₂₀F₃N
Molecular Weight:379.425
Hs Code.:

Synonyms:(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

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Technology Process of (1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

There total 3 articles about (1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 356762-89-5
N-(1,1-diphenyl-3-butenyl)amine

: (S)-1,1-diphenyl-N-(1-(4-(trifluoromethyl)phenyl)but-3-en-1-yl)methanimine

: 1123309-26-1
(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

Guidance literature:: With (R)-3,3'-bis-(2-naphthyl)octahydrobinol; In tert-butyl methyl ether; at 50 ℃; for 48h; optical yield given as %ee; enantioselective reaction; Molecular sieve;
DOI:10.1002/anie.200803610

Reference yield:

: allyl (E)-2-((4-(trifluoromethyl)benzylidene)amino)-2,2-diphenyl-2-acetate

: (S)-1,1-diphenyl-N-(1-(4-(trifluoromethyl)phenyl)but-3-en-1-yl)methanimine

: 1123309-26-1
(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,1'-bis[(S)-4,5-dihydro-3H-binaphtho[2,1-c:1',2'-e]phosphino]ferrocene; In dimethyl sulfoxide; at 25 ℃; for 24h; Overall yield = 79 %; Overall yield = 67.7 mg; enantioselective reaction; Inert atmosphere;
DOI:10.1021/acs.joc.8b00491

Reference yield:

: C₂₅H₂₀F₃NO₂

: (S)-1,1-diphenyl-N-(1-(4-(trifluoromethyl)phenyl)but-3-en-1-yl)methanimine

: 1123309-26-1
(1R)-N-(diphenylmethylene)-1-[4-(trifluoromethyl)phenyl]but-3-en-1-amine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; C₅₄H₄₂FeP₂; In dimethyl sulfoxide; at 25 ℃; for 24h; Solvent; Sealed tube; Glovebox; Inert atmosphere;
DOI:10.1021/acs.joc.9b01293