3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Base Information

Chemical Name:3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin
CAS No.:116611-92-8
Molecular Formula:C₂₅H₂₂O₅
Molecular Weight:402.447
Hs Code.:

Synonyms:3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Suppliers and Price of 3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

There total 4 articles about 3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 116589-44-7
7-hydroxy-8-(4'-methoxycinnamoyl)-4-phenylcoumarin

: 116611-92-8
3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 6h;

Reference yield:

: 57391-60-3
8-acetyl-7-methoxy-4-phenyl-chromen-2-one

: 116611-92-8
3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / KOH / ethanol / 6 h / 35 - 40 °C

2: 70 percent / AlCl₃ / acetonitrile / 1.) rt, 30 min, 2.) 40-45 deg C, 8 h

3: 65 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h

With potassium hydroxide; aluminium trichloride; hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; acetonitrile;

Reference yield:

: 116589-43-6
7-methoxy-8-(4'-methoxycinnamoyl)-4-phenylcoumarin

: 116611-92-8
3,4-dihydro-8-(α,β-dihydro-4'-methoxycinnamoyl)-7-hydroxy-4-phenylcoumarin

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / AlCl₃ / acetonitrile / 1.) rt, 30 min, 2.) 40-45 deg C, 8 h

2: 65 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h

With aluminium trichloride; hydrogen; palladium on activated charcoal; In ethyl acetate; acetonitrile;