5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

Base Information

Chemical Name:5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one
CAS No.:120129-31-9
Molecular Formula:C₁₃H₁₇NO₄S₂
Molecular Weight:315.414
Hs Code.:

Synonyms:5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

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Chemical Property of 5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

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Technology Process of 5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

There total 5 articles about 5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 118878-26-5
(2,2,2-Trichloro-acetyl)-carbamic acid (E)-(S)-1-methyl-3-methylsulfanyl-3-(toluene-4-sulfonyl)-allyl ester

: 120129-31-9
5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; at 25 ℃; for 3h;
DOI:10.1016/0040-4039(88)85102-5

Reference yield:

: 118878-26-5
(2,2,2-Trichloro-acetyl)-carbamic acid (E)-(S)-1-methyl-3-methylsulfanyl-3-(toluene-4-sulfonyl)-allyl ester

: 118878-22-1,118878-27-6,120129-31-9
(4R,5S)-5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; for 2h; Yield given;
DOI:10.1016/0040-4039(88)85103-7

Reference yield:

: 59662-65-6
methylthiomethyl p-tolyl sulfone

: 118878-22-1,118878-27-6,120129-31-9
(4R,5S)-5-Methyl-4-[methylsulfanyl-(toluene-4-sulfonyl)-methyl]-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi, 2.) methanesulfonyl chloride / 1.) THF, -78 deg C, 2.) pyridine, 0 deg C - room temperature

2: 1 N HCl / methanol

3: CH₂Cl₂ / 0 °C

4: K₂CO₃ / methanol; CH₂Cl₂ / 2 h

With hydrogenchloride; n-butyllithium; potassium carbonate; methanesulfonyl chloride; In methanol; dichloromethane;
DOI:10.1016/0040-4039(88)85103-7